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Figure 1.
IG. . The progress of the partial refinement f tosyl-y-CHT nd, subsequently, native yCHT is
shown. he left-hand curve refers to the osyl-y-CHT (2.7 ) and the right-hand one to the naive y-HT
(1.9A). The refinement method is indicated along the horizontal bar in the igure sing the code:
RS(m.i.r.). real-space mehod on .i.r. aps; S(ZF,-FJ. real-space method n 2F- F, aps; DDF,
differential difference Fourier; Lt51, least-squares series 1; S2, least-squares series 2. The -factor is
defined in the onventional manner as H = [[F,,[ - IF,II/x IF,], ere F, s an observed structure factor
and F, is calculated tructure factor.
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