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Figure 2.
Figure 2. Summary of sequential and medium-range connectivities
for AP-B at pH 4.5 and 298 K. Filled bars indicate the
sequential connectivities, with the heights of the bars
indicating their strength. Medium-range connectivities are also
shown, but the heights of the bars do not indicate the
strength of these interactions. Hatched bars correspond to
sequential d[αδ] connectivities for prolines, except for
Gly40–Pro41 where a d[αα] connectivity was observed. A star
(*) indicates that the cross-peak could not be observed due to
peak overlap or water suppression. Values of ^3JHN-CaH >8 Hz are
indicated by ↑ while values <5.5 Hz are indicated by ↓.
Slowly exchanging amide protons (visible in at least two
consecutive TOCSY spectra recorded after dissolution in ^2H[2]O)
are indicated by filled circles and those with intermediate
exchange rates (visible in only the first TOCSY spectrum after
dissolution in ^2H[2]O) by open circles. Figure 2. Summary of
sequential and medium-range connectivities for AP-B at pH 4.5
and 298 K. Filled bars indicate the sequential connectivities,
with the heights of the bars indicating their strength.
Medium-range connectivities are also shown, but the heights of
the bars do not indicate the strength of these interactions.
Hatched bars correspond to sequential d[αδ] connectivities for
prolines, except for Gly40–Pro41 where a d[αα] connectivity
was observed. A star (*) indicates that the cross-peak could not
be observed due to peak overlap or water suppression. Values of
^3JHN-CaH >8 Hz are indicated by ↑ while values <5.5 Hz are
indicated by ↓. Slowly exchanging amide protons (visible in at
least two consecutive TOCSY spectra recorded after dissolution
in ^2H[2]O) are indicated by filled circles and those with
intermediate exchange rates (visible in only the first TOCSY
spectrum after dissolution in ^2H[2]O) by open circles.
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